Testosterone phenylpropionate synthesis
- Product Name:Testosterone phenylpropionate
- CAS Number:1255-49-8
- Molecular formula:C28H36O3
- Molecular Weight:420.58
In a 100 ml reaction flask, 0.397 g (3 mmol) of cinnamaldehyde was added.0.411g (1.5mmol) Nandrolone, 0.06g (0.3mmol) [Bmim][OAc] catalyst, 10ml 1,4-dioxane, heated to 120 ° C and then reacted for 2h, after the reaction was completed, cooled to room temperature, added 30 ml of water and 20 ml of ethyl acetate were extracted, and the phases were allowed to stand. The organic phase was concentrated and crystallized to obtain the target product. The yield was 64%.
58-22-0
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104-55-2
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1255-49-8
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Yield:1255-49-8 64%
Reaction Conditions:
with 3-butyl-1-methylimidazolium acetate in 1,4-dioxane at 120; for 2 h;
Steps:
7
In a 100 ml reaction flask, 0.397 g (3 mmol) of cinnamaldehyde was added.0.411g (1.5mmol) Nandrolone, 0.06g (0.3mmol) [Bmim][OAc] catalyst, 10ml 1,4-dioxane, heated to 120 ° C and then reacted for 2h, after the reaction was completed, cooled to room temperature, added 30 ml of water and 20 ml of ethyl acetate were extracted, and the phases were allowed to stand. The organic phase was concentrated and crystallized to obtain the target product. The yield was 64%.
References:
CN109678718,2019,A Location in patent:Paragraph 0036
![Androst-4-en-3-one, 17-[[(triphenylphosphoranylidene)acetyl]oxy]-, (17β)- (9CI)](/CAS/20210305/GIF/131447-69-3.gif)
131447-69-3
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100-51-6
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1255-49-8
260 suppliers
$17.00/5mg
58-22-0
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645-45-4
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1255-49-8
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