TERT-BUTYL 3-METHYL-4-NITROPHENYLCARBAMATE synthesis
- Product Name:TERT-BUTYL 3-METHYL-4-NITROPHENYLCARBAMATE
- CAS Number:1380445-45-3
- Molecular formula:C12H16N2O4
- Molecular Weight:252.27
24424-99-5
840 suppliers
$13.50/25G
611-05-2
155 suppliers
$16.00/1g
1380445-45-3
24 suppliers
inquiry
Yield:1380445-45-3 54%
Reaction Conditions:
Stage #1: di-tert-butyl dicarbonate;4-nitro-3-methylanilinewith dmap in acetonitrile; for 0.0833333 h;
Stage #2: with triethylamine in acetonitrile;
References:
Wylie, Laura;Innocenti, Paolo;Whelligan, Daniel K.;Hoelder, Swen [Organic and Biomolecular Chemistry,2012,vol. 10,# 22,p. 4441 - 4447] Location in patent:supporting information; experimental part