tert-butyl 3,5-dibroMobenzoate synthesis
- Product Name:tert-butyl 3,5-dibroMobenzoate
- CAS Number:422569-46-8
- Molecular formula:C11H12Br2O2
- Molecular Weight:336.02
626-39-1
471 suppliers
$5.00/5g
24424-99-5
840 suppliers
$13.50/25G
422569-46-8
15 suppliers
inquiry
Yield:422569-46-8 97%
Reaction Conditions:
Stage #1: 1,3,5-trisbromobenzenewith n-butyllithium;butyl magnesium bromide in tetrahydrofuran;hexane;toluene at -10;
Stage #2: di-tert-butyl dicarbonate in tetrahydrofuran;hexane;toluene at -10;
Stage #3: with citric acid in tetrahydrofuran;hexane;toluene;Further stages.;
References:
Li, Hongmei;Balsells, Jaume [Tetrahedron Letters,2008,vol. 49,# 12,p. 2034 - 2037]
24424-99-5
840 suppliers
$13.50/25G
618-58-6
270 suppliers
$6.00/5g
422569-46-8
15 suppliers
inquiry