Spiroglumide synthesis
- Product Name:Spiroglumide
- CAS Number:137795-35-8
- Molecular formula:
- Molecular Weight:0
![8-AZASPIRO[4.5]DECANE](/CAS/GIF/176-64-7.gif)
176-64-7
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137795-35-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 1.) triethylamine, ethyl chloroformate / 1.) THF, -10 deg C, 15 min, 2.)a) THF, -10 deg C, 1 h, b) RT, 3 h
2: H2, H2O / 10percent Pd/activated charcoal / methanol / 2 h / 760 Torr / Ambient temperature
3: aq. NaOH / tetrahydrofuran / 3 h / Ambient temperature
References:
Makovec, Francesco;Peris, Walter;Revel, Laura;Giovanetti, Roberto;Mennuni, Laura;Rovati, Lucio C. [Journal of Medicinal Chemistry,1992,vol. 35,# 1,p. 28 - 38]
59486-73-6
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$23.00/1g
137795-35-8
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![(R)-benzyl 4-(((benzyloxy)carbonyl)amino)-5-oxo-5-(8-azaspiro[4.5]decan-8-yl)pentanoate](/CAS/20180601/GIF/137822-90-3.gif)
137822-90-3
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![(R)-4-amino-5-oxo-5-(8-azaspiro[4.5]decan-8-yl)pentanoic acid](/CAS/20180529/GIF/137795-97-2.gif)