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ChemicalBook CAS DataBase List Sodium Methoxide
124-41-4

Sodium Methoxide synthesis

7synthesis methods
-

Yield:-

Steps:

1 Examples; Example 1 : 2-Nitro-5-chloroaniline

Examples Example 1 : 2-Nitro-5-chloroaniline : A solution of metallic sodium(0.012 g, 0.52mmol) in 44NIT of absolute methanol was added to 2-NITRO-5-CHLORO ACETANILIDE (4. 8 G, 23MMOL). The solution was boiled under reflux for 3h and then the solvent was evaporated to obtain the desired yellow crystalline product in 98% yield. m. p. 126-129'C

References:

WO2004/63170,2004,A1 Location in patent:Page 7

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