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ChemicalBook CAS DataBase List SEPTIDE
79775-19-2

SEPTIDE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 6 steps
1: N-methylmorpholine / dimethylformamide / 0.03 h / -20 °C
2: N-methylmorpholine, hexamethylphosphoric acid triamide / dimethylformamide / 2 h / -20 °C
3: 89 percent / 1 N HCl / acetic acid / 0.5 h / Ambient temperature
4: N-methylmorpholine / dimethylformamide / 2 h / -20 °C
5: 95 percent / 1 N HCl / acetic acid / 0.5 h / Ambient temperature
6: N-methylmorpholine / dimethylformamide / 2 h / -20 °C

References:

Laufer, Ralph;Gilon, Chaim;Chorev, Michael;Selinger, Zvi [Journal of Medicinal Chemistry,1986,vol. 29,# 7,p. 1284 - 1288]

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