(S)-2-amino-3-cyclohexyl-2-methylpropanoic acid synthesis
- Product Name:(S)-2-amino-3-cyclohexyl-2-methylpropanoic acid
- CAS Number:942143-63-7
- Molecular formula:C10H19NO2
- Molecular Weight:185.2634
70869-86-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 - 0 °C / Inert atmosphere
1.2: 3 h / -50 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; water / 12 h / 23 °C / Inert atmosphere
3.1: water / 1,4-dioxane / 2 h / 100 °C / Inert atmosphere
References:
Hugelshofer, Cedric L.;Mellem, Kevin T.;Myers, Andrew G. [Organic Letters,2013,vol. 15,# 12,p. 3134 - 3137]
100-49-2
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