RARECHEM AL BI 0711 synthesis
- Product Name:RARECHEM AL BI 0711
- CAS Number:55211-85-3
- Molecular formula:C10H12O3
- Molecular Weight:180.2
Yield:-
Reaction Conditions:
with HNO3 at 60; under 760.051 Torr; for 3 h;
Steps:
5.2 (2) preparation step 2:
In the reactor, 1 mole of compound 2 in the above formula was reacted with nitric acid; the substance ratio of compound 2 and nitric acid was 1:1.2; the solvent was ethanol, the reaction temperature was 60°C, the reaction pressure was normal pressure, and the reaction time For 3 hours, the reaction was completed, and the reaction was continued to complete, After the reaction was completed, the solvent was removed and the ester of 3-methylsalicylic acid was obtained.
References:
CN114835574,2022,A Location in patent:Paragraph 0110-0111; 0115-0117
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