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ChemicalBook CAS DataBase List (R)-(+)-2,2'-BIS(METHOXYMETHOXY)-1,1'-BINAPHTHYL
173831-50-0

(R)-(+)-2,2'-BIS(METHOXYMETHOXY)-1,1'-BINAPHTHYL synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: iron(III) chloride hexahydrate / water / 3 h / 20 - 50 °C / Inert atmosphere
2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2.2: 4.5 h / 0 - 20 °C / Inert atmosphere

References:

Lv, Na;Xie, Meilan;Gu, Weibing;Ruan, Huanyang;Qiu, Song;Zhou, Chunshan;Cui, Zheng [Organic Letters,2013,vol. 15,# 10,p. 2382 - 2385]

150587-19-2 Synthesis
Hypochlorous acid, methoxymethyl ester (9CI)

150587-19-2
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602-09-5 Synthesis
1,1'-Bi-2-naphthol

602-09-5
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