Quinagolide synthesis
- Product Name:Quinagolide
- CAS Number:87056-78-8
- Molecular formula:C20H33N3O3S
- Molecular Weight:395.56
87056-65-3
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87056-78-8
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: H2 / 10percent Pd/C / propan-1-ol / Ambient temperature
2: 80 percent / H2NNH2*H2O / methanol / 20 h / 50 °C
3: NOCl / tetrahydrofuran / 1 h / Heating
4: aq. HCl / tetrahydrofuran / 1 h / Heating; 1.) THF, reflux, 1 h, 2.) THF, reflux, 1 h
5: 87 percent / Et3N / CHCl3 / 50 °C
6: BBr3 / CH2Cl2 / 4 h / -10 °C
References:
Nordmann;Petcher [Journal of Medicinal Chemistry,1985,vol. 28,# 3,p. 367 - 375]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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87056-78-8
15 suppliers
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1000210-73-0
0 suppliers
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87056-78-8
15 suppliers
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1000210-73-0
0 suppliers
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87056-78-8
15 suppliers
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1000210-73-0
0 suppliers
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87056-78-8
15 suppliers
inquiry