p-(2-methoxyethyl)anisole synthesis
- Product Name:p-(2-methoxyethyl)anisole
- CAS Number:80314-58-5
- Molecular formula:C10H14O2
- Molecular Weight:166.22
Yield:80314-58-5 95%
Reaction Conditions:
with Amberlyst 15 for 12 h;Reflux;
Steps:
General procedure for methylation of phenethyl alcohols in Amberlyst 15
General procedure: Amberlyst 15 (0.05 mmol, 11 mg) was added to asolution of the alcohol (1.0 mmol) in DMC (5 mL). The reaction mixture wasstirred at reflux for 36 hours adding Amberlyst 15 every 12 hours. The organicsolvent was filtered and evaporated as an azeotropic mixture with MeOH(DMC:MeOH 1:3) to obtain the product as a gummy oil.
References:
Barontini;Proietti Silvestri;Nardi;Bovicelli;Pari;Gallucci;Spezia;Righi [Tetrahedron Letters,2013,vol. 54,# 37,p. 5004 - 5006] Location in patent:supporting information
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