Oxapium iodide synthesis
- Product Name:Oxapium iodide
- CAS Number:6577-41-9
- Molecular formula:C22H34INO2
- Molecular Weight:471.4153
![Piperidine, 1-[(2-cyclohexyl-2-phenyl-1,3-dioxolan-4-yl)methyl]-](/CAS/20180601/GIF/65471-77-4.gif)
Yield:6577-41-9 82.1%
Reaction Conditions:
in ethanol at 20; for 28 h;Time;
Steps:
5 S3, preparation Oshathium iodide:
50 parts of 2-phenyl-2-cyclohexyl-4-pipe obtained in S2 were added in parts by weight Pyridine-1,3-dioxolane was added to 130 parts of ethanol was dissolved, methyl iodide added 26 parts, stirred at room temperature for 28h, Distillation under reduced pressure to obtain material C; the material C isopropanol added recrystallization, and dried to give osmium iodonium iodide.
References:
CN106560469,2017,A Location in patent:Paragraph 0031; 0036; 0041; 0046; 0051
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