午夜插插,噜噜噜影院,啪啪伊人网,欧美熟夫,景甜吻戏视频,男人强操性感蕾丝美女视频在线网站,日本美女跳舞视频

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List o-Tolyl Trifluoromethanesulfonate
66107-34-4

o-Tolyl Trifluoromethanesulfonate synthesis

6synthesis methods
-

Yield:-

Reaction Conditions:

with triethylamine in dichloromethane at 0; for 24 h;

Steps:

Phenyl Trifluoromethanesulfonate; Typical Procedure

General procedure: A mixture of phenol (0.45 g, 5 mmol), trifluoromethanesulfonyl chloride (0.8 mL, 7.5 mmol) and Et3N (1.4 mL, 10 mmol) in THF (30 mL) was stirred at 0 °C for 24 h. The solvent was evaporated and to the resulting residue were added H2O (20 mL) and EtOAc (20 mL). The organic phase was decanted and dried (anhyd Na2SO4). Evaporation of the solvent and purification by column chromatography on silica gel (hexane/EtOAc, 4:1) gave the pure triflate in 85% yield (191 mg).

References:

Rostami, Abed;Rostami, Amin;Ghaderi, Arash;Gholinejad, Mohammad;Gheisarzadeh, Sajedeh [Synthesis,2017,vol. 49,# 22,art. no. SS-2016-N0842-OP,p. 5025 - 5038]

o-Tolyl Trifluoromethanesulfonate Related Search: