N-PHENYLBENZOTRIAZOLEMETHANAMINE synthesis
- Product Name:N-PHENYLBENZOTRIAZOLEMETHANAMINE
- CAS Number:62001-29-0
- Molecular formula:C13H12N4
- Molecular Weight:224.26
95-14-7
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50-00-0
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62-53-3
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62001-29-0
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Yield:62001-29-0 90%
Reaction Conditions:
in methanol at 20; for 2 h;
Steps:
Synthesis of Compound N-((1H-benzo[d][1,2,3]triazole)-1-methyl)aniline
Weigh benzotriazole (5mmol, 596mg), aniline (5mmol, 466mg), 40% formic acid (5mmol,375mg ) placed in 100mL round-bottomed flask , was added 60mL of methanol , stirred for 2 hours at room temperature , there are a lot of white solid precipitated pumpingFiltered , the filter cake washed with cold methanol , and dried to give the title compound . White solid , mass : 1.9g ( yield: 90% )
References:
CN102688233,2016,B Location in patent:Paragraph 0075-0077
95-14-7
882 suppliers
$6.00/100g
62-53-3
660 suppliers
$10.00/1g
62001-29-0
7 suppliers
$130.00/50mg
28539-02-8
151 suppliers
$6.00/1g
62-53-3
660 suppliers
$10.00/1g
62001-29-0
7 suppliers
$130.00/50mg