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ChemicalBook CAS DataBase List N,N-Diisopropyl-P,P-diphenylphosphinicamide
131173-04-1

N,N-Diisopropyl-P,P-diphenylphosphinicamide synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: copper(I) tetrakis(acetonitrile)tetrafluoroborate; Cs2CO3 / tetrahydrofuran / 12 h / 20 °C / Schlenk technique; Glovebox; Inert atmosphere
2: dihydrogen peroxide / tetrahydrofuran; water monomer / 0.5 h / 20 °C / Schlenk technique; Glovebox; Inert atmosphere

References:

Li, Yan-Bo;Tian, Hu;Xiao, Jun-Zhao;Yin, Liang;Zhang, Shuai [Angewandte Chemie - International Edition,2022,vol. 61,# 13,art. no. E202117760][Angew. Chem.,2022,vol. 134,# 13]