N-Carbethoxyphthalimide synthesis
2synthesis methods
- Product Name:N-Carbethoxyphthalimide
- CAS Number:22509-74-6
- Molecular formula:C11H9NO4
- Molecular Weight:219.19
N-Carbethoxyphthalimide is prepared for: addition of Ethyl Chloroformate to a cold solution of Phthalimide and Triethylamine in DMF; alkylation of potassium phthalimide with ethyl chloroformate.
Yield:22509-74-6 96%
Reaction Conditions:
with 18-crown-6 ether in toluene at 90; for 1 h;
References:
Soai, Kenso;Ookawa, Atsuhiro;Kato, Kyoko [Bulletin of the Chemical Society of Japan,1982,vol. 55,# 5,p. 1671 - 1672]