N-BSMOC-L-VALINE synthesis
- Product Name:N-BSMOC-L-VALINE
- CAS Number:197245-17-3
- Molecular formula:C15H17NO6S
- Molecular Weight:339.36
134996-50-2
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$37.39/1g
197245-17-3
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$497.51/5MG
Yield:-
Steps:
Multi-step reaction with 2 steps
1: 36.1 g / tetrahydrofuran / -30 - 20 °C
2: 1.) Me3SiCl, 2.) i-Pr2NEt / 1.) CH2Cl2, reflux, 1 h, 2.) 0 deg C 20 min,; room temperature, 1-1.5 h
References:
Carpino, Louis A.;Ismail, Mohamed;Truran, George A.;Mansour;Iguchi, Shin;Ionescu, Dumitru;El-Faham, Ayman;Riemer, Christoph;Warrass, Ralf [Journal of Organic Chemistry,1999,vol. 64,# 12,p. 4324 - 4338]
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197245-17-3
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17890-56-1
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197245-17-3
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197245-17-3
15 suppliers
$497.51/5MG