N-(2,6-dimethylphenyl)propanamide synthesis
- Product Name:N-(2,6-dimethylphenyl)propanamide
- CAS Number:25404-20-0
- Molecular formula:C11H15NO
- Molecular Weight:177.24
28556-81-2
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Yield:25404-20-0 10%
Reaction Conditions:
Stage #1: 2,6-dimethylphenylisocyanatewith [Rh(OH)(cod)]2 in tetrahydrofuran at 20; for 0.0833333 h;Inert atmosphere;
Stage #2: ethylzinc iodide in tetrahydrofuran at 20; for 24 h;Inert atmosphere;
References:
Fouad, Moustafa H.;Ismailani, Uzair S.;Mair, Braeden A.;Munch, Maxime;Rotstein, Benjamin H. [Organic Letters,2020,vol. 22,# 7,p. 2746 - 2750] Location in patent:supporting information
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