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ChemicalBook CAS DataBase List MK-1775
955365-80-7

MK-1775 synthesis

5synthesis methods
26218-75-7 Synthesis
Methyl 6-bromopicolinate

26218-75-7
238 suppliers
$9.00/1g

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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: diethyl ether / 0.08 h / 20 °C / Inert atmosphere
2.1: potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide / 1,4-dioxane / 18 h / 80 - 95 °C
3.1: 3-chloro-benzenecarboperoxoic acid / toluene / 1 h / 20 °C
3.2: 18 h / 20 °C

References:

Matheson, Christopher J.;Casalvieri, Kimberly A.;Backos, Donald S.;Reigan, Philip [ChemMedChem,2018,vol. 13,# 16,p. 1681 - 1694]

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