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ChemicalBook CAS DataBase List Methylene dithiocyanate
6317-18-6

Methylene dithiocyanate synthesis

3synthesis methods
Synthesis of methylene dithiocyanate: under pressure, add excess sodium thiocyanate (or sodium thiocyanate) and dichloromethane into the reaction kettle, start stirring, and heat up to 80-100°C at the same time. After the reaction is completed, dichloromethane is recovered, and the solid-liquid two phases are separated to obtain a crude methylene dithiocyanate.
-

Yield:-

Reaction Conditions:

with ethanol

References:

Lermontow [Chemische Berichte,1874,vol. 7,p. 1282]

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