METHYL-D3 ACETATE synthesis

4synthesis methods

Product Name:METHYL-D3 ACETATE
CAS Number:24704-57-2
Molecular formula:C3H3D3O2
Molecular Weight:77.1

811-98-3
211 suppliers
$18.69/1g

141-78-6 Synthesis

141-78-6
634 suppliers
$22.37/250ml

925-93-9 Synthesis

925-93-9
80 suppliers
$58.50/25ml

24704-57-2
14 suppliers
$502.62/5MG

Yield:-

Reaction Conditions:

with N-ethyl-N,N-diisopropylamine at 21.5;Kinetics;

Steps:

7

General procedure: For each kinetics trial, 1.00 mL of a 1.03 M (i-Pr)₂NEt/MeOH-d₄ solution was added to a measured amount of ester so that the initial concentration of ester was about 0.1 M. Kinetics data were collected as a series of signal integrations with a Bruker Avance DPX-300 NMR spectrometer. Each rate constant was calculated by the least-squares method for the simple linear regression equation ln (%ROAc) = -kt + C. Each value in Table 2 is the average of at least two determinations.

References:

Hankins, Jamilah N.;Gouws, Michele;Mahajer, Amir;Kim, Ethan S.;Gwaltney, Kevin P.;Haseltine, John [Tetrahedron Letters,2012,vol. 53,# 19,p. 2450 - 2453] Location in patent:experimental part

811-98-3
211 suppliers
$18.69/1g

75-36-5 Synthesis