Methyl cyanoformate synthesis
- Product Name:Methyl cyanoformate
- CAS Number:17640-15-2
- Molecular formula:C3H3NO2
- Molecular Weight:85.06
280-57-9
573 suppliers
$5.00/5g
7677-24-9
385 suppliers
$19.00/5g
79-22-1
2 suppliers
$38.00/1000g
17640-15-2
60 suppliers
$85.00/250mg
Yield:-
Steps:
4 Methyl Cyanoformate
EXAMPLE 4 Methyl Cyanoformate To a mixture of methyl chloroformate (4.73 g; 0.05 mol) and 1,4-diazabicyclo [2.2.2] octane (5 mg; 0.05 mmol) was added dropwise trimethylsilyl nitrile (5.0 g; 0.05 mol) and the mixture maintained at 20°-25° C. for about 1-2 hr with stirring. The resulting methyl cyanoformate was identified by gas chromatography and spectroscopy. 1 H-NMR: δ4.0, s(3H); IR: 2250 cm-1 (CN), 1750 cm-1 (CO).
References:
Creanova Inc. US5852207, 1998, A
151-50-8
4 suppliers
$36.39/100g
79-22-1
2 suppliers
$38.00/1000g
17640-15-2
60 suppliers
$85.00/250mg
143-33-9
5 suppliers
$10.00/1g
79-22-1
2 suppliers
$38.00/1000g
17640-15-2
60 suppliers
$85.00/250mg
1738-36-9
150 suppliers
$20.00/5g
17640-15-2
60 suppliers
$85.00/250mg
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