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ChemicalBook CAS DataBase List methyl 7-oxoheptanoate
35376-00-2

methyl 7-oxoheptanoate synthesis

15synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 9 steps
1.1: 96 percent / potassium carbonate / dimethylformamide / 20 °C
2.1: potassium carbonate; CuCl; Bu4NI / dimethylformamide / 0.17 h / 20 °C
2.2: dimethylformamide
3.1: 8.3 g / OsO4; N-methylmorpholine N-oxide / H2O; tetrahydrofuran; acetone / 10 h / 20 °C
4.1: 97 percent / hydrogen / Lindlar catalyst / ethyl acetate / 4 h
5.1: 82 percent / p-TsOH / acetone / 2 h / 20 °C
6.1: 97 percent / hydrogen / Pd/C / ethyl acetate / 3 h
7.1: 80 percent / DCC; 4-(dimethylamino)pyridine / CH2Cl2 / 3 h / 20 °C
8.1: 77 percent / p-TsOH / methanol / 4 h / 20 °C
9.1: 78 percent / aq. NaIO4 / CH2Cl2 / 0.33 h / 20 °C

References:

Wen, Shijun;Carey, Krystle L.;Nakao, Yoichi;Fusetani, Nobuhiro;Packham, Graham;Ganesan [Organic Letters,2007,vol. 9,# 6,p. 1105 - 1108]

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