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ChemicalBook CAS DataBase List Methyl 2-fluoro-6-formylbenzoate
1256593-43-7

Methyl 2-fluoro-6-formylbenzoate synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 20 - 85 °C / Inert atmosphere
1.2: 1 h / 100 °C
2.1: potassium carbonate / acetone / 2 h / 20 °C / Inert atmosphere
2.2: 1 h / Reflux

References:

He, Yuwei;Cheng, Chuyu;Chen, Bin;Duan, Kun;Zhuang, Yue;Yuan, Bo;Zhang, Meisan;Zhou, Yougui;Zhou, Zihong;Su, Yu-Jun;Cao, Rihui;Qiu, Liqin [Organic Letters,2014,vol. 16,# 24,p. 6366 - 6369]

820236-81-5 Synthesis
Methyl 2-bromo-6-fluorobenzoate

820236-81-5
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Methyl 2-fluoro-6-formylbenzoate

1256593-43-7
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