METHYL 2,2':6',2''-TERPYRIDINE-4'-CARBOXYLATE synthesis
- Product Name:METHYL 2,2':6',2''-TERPYRIDINE-4'-CARBOXYLATE
- CAS Number:247058-06-6
- Molecular formula:C17H13N3O2
- Molecular Weight:291.3
1122-62-9
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247058-06-6
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Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: 100 percent / 15 percent NaOH / methanol / 2 h / 0 °C
2.1: 60 percent / Et2NH / methanol / 48 h / 20 °C
3.1: AcONH4 / ethanol / 5 h
4.1: 68 percent / KMnO4; pyridine / H2O / 24 h / 20 °C
5.1: POCl3; PCl5 / 1.5 h / Heating
5.2: 3 percent / 0.5 h / Heating
References:
Raboin;Kirsch;Beley [Journal of Heterocyclic Chemistry,2000,vol. 37,# 5,p. 1077 - 1080]
67-56-1
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148332-36-9
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247058-06-6
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148332-36-9
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74-88-4
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247058-06-6
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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247058-06-6
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375382-77-7
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247058-06-6
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