Hexetidine synthesis

1synthesis methods

Product Name:Hexetidine
CAS Number:141-94-6
Molecular formula:C21H45N3
Molecular Weight:339.6

Hexetidine is prepared by hydrogenation under pressure of 1,3- bis(2-ethylhexyl)-5-methyl-4-nitrohexahydropyriminine at 100°C using Raney nickel as a catalyst.

1,3-bis(2-ethylhexyl)hexahydro-5-methyl-5-nitropyrimidine

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Yield:-

Reaction Conditions:

with methanol;nickel at 100; under 51485.6 Torr;Hydrogenation;

References:

Senkus [Journal of the American Chemical Society,1946,vol. 68,p. 1611][Chem.Abstr.,1946,p. 1889]

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