Fmoc-L-beta-homoglutamic acid 6-tert-butyl ester synthesis

2synthesis methods

Product Name:Fmoc-L-beta-homoglutamic acid 6-tert-butyl ester
CAS Number:203854-49-3
Molecular formula:C25H29NO6
Molecular Weight:439.5

71989-18-9 Synthesis

71989-18-9
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Fmoc-L-beta-homoglutamic acid 6-tert-butyl ester

203854-49-3
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$27.00/100mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: Fmoc-Cl; N-methylmorpholine / tetrahydrofuran / 0.17 h / -15 °C
1.2: 78 percent / tetrahydrofuran; diethyl ether / 0 - 20 °C
2.1: 78 percent / silver benzoate / dioxane; H₂O / 0.02 h / microwave irradiation

References:

Kantharaju;Suresh Babu, Vommina V. [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2004,vol. 43,# 10,p. 2152 - 2158]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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203854-49-3
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$27.00/100mg

References

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