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ChemicalBook CAS DataBase List FENITROTHION-O-ANALOG
2255-17-6

FENITROTHION-O-ANALOG synthesis

2synthesis methods
Fenitrothion-oxon can be prepared by nitrifying and oxidizing m-cresol to 3-methyl-4-nitrophenol, and then reacting with dimethylphosphoryl thiochloride.
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Yield:2255-17-6 100%

Reaction Conditions:

with 3,3-dimethyldioxirane in dichloromethane;acetone for 0.0833333 h;Ambient temperature;

References:

Sanchez-Baeza, Francisco;Durand, Gael;Barcelo, Damia;Messeguer, Angel [Tetrahedron Letters,1990,vol. 31,# 23,p. 3359 - 3362]

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