Ethyl tiglate synthesis
- Product Name:Ethyl tiglate
- CAS Number:5837-78-5
- Molecular formula:C7H12O2
- Molecular Weight:128.17
105-37-3
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5837-78-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 1.) diisopropylamine, n-butyllithium / 1.) THF, hexane, -78 deg C, 30 min; 2.) -78 deg C, 15 min; room temp., 1 h
2: butyllithium / hexane; diethyl ether / -40 - -30 °C
3: triethylamine / methanol / 6 h / Heating
References:
Slougui, Nasser;Rousseau, Gerard;Conia, Jean-Marie [Synthesis,1982,# 1,p. 58 - 60]
80-59-1
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64-17-5
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5837-78-5
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547-65-9
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64-17-5
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22122-36-7
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5837-78-5
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![Silane, [(1-ethoxy-1-propenyl)oxy]trimethyl-](/CAS/20180601/GIF/80675-53-2.gif)
80675-53-2
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5837-78-5
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609-14-3
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5837-78-5
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