ethyl (E)-o-methoxycinnamate synthesis
- Product Name:ethyl (E)-o-methoxycinnamate
- CAS Number:24393-54-2
- Molecular formula:C12H14O3
- Molecular Weight:206.24
Yield:24393-54-2 100%
Reaction Conditions:
Stage #1: diethoxyphosphoryl-acetic acid ethyl esterwith sodium hydride in tetrahydrofuran;mineral oil at 23; for 0.5 h;Inert atmosphere;Cooling with ice;
Stage #2: ortho-anisaldehyde in tetrahydrofuran;mineral oil at 0 - 23; for 0.666667 h;Inert atmosphere;
References:
Kaga, Atsushi;Hayashi, Hirohito;Hakamata, Hiroyuki;Oi, Miku;Uchiyama, Masanobu;Takita, Ryo;Chiba, Shunsuke [Angewandte Chemie - International Edition,2017,vol. 56,# 39,p. 11807 - 11811][Angew. Chem.,2017,vol. 129,p. 11969 - 11973] Location in patent:supporting information
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