Ethyl 4-amino-1-piperidinecarboxylate synthesis
- Product Name:Ethyl 4-amino-1-piperidinecarboxylate
- CAS Number:58859-46-4
- Molecular formula:C8H16N2O2
- Molecular Weight:172.22
29976-53-2
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58859-46-4
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Yield: 93%
Reaction Conditions:
Stage #1:N-ethoxycarbonyl-4-piperidone with titanium(IV) isopropylate;ammonia in ethanol at 25; for 6 h;
Stage #2: with sodium tetrahydroborate in ethanol at 25; for 3 h;Further stages.;
References:
Miriyala, Bruhaspathy;Bhattacharyya, Sukanta;Williamson, John S. [Tetrahedron,2004,vol. 60,# 7,p. 1463 - 1471]