ETHYL 2,6-DIMETHYLBENZOYLFORMATE synthesis
- Product Name:ETHYL 2,6-DIMETHYLBENZOYLFORMATE
- CAS Number:698392-47-1
- Molecular formula:C12H14O3
- Molecular Weight:206.24
6781-98-2
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4755-77-5
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698392-47-1
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Yield:698392-47-1 99%
Reaction Conditions:
Stage #1: 2,6-dimethyl-1-chlorobenzenewith lithium in diethyl ether at 3 - 6;
Stage #2: with copper(l) cyanide in tetrahydrofuran;diethyl ether at -80 - -25; for 0.416667 h;
Stage #3: Ethyl oxalyl chloride in tetrahydrofuran;diethyl ether at -80;
References:
Screttas, Constantinos G.;Steele, Barry R.;Micha-Screttas, Maria;Heropoulos, Georgios A. [Organic Letters,2012,vol. 14,# 22,p. 5680 - 5683] Location in patent:supporting information
2039-90-9
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698392-47-1
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608-28-6
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698392-47-1
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19447-06-4
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698392-47-1
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