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ChemicalBook CAS DataBase List DIISOPROPYLSILYL BIS(TRIFLUOROMETHANESULFONATE)
85272-30-6

DIISOPROPYLSILYL BIS(TRIFLUOROMETHANESULFONATE) synthesis

2synthesis methods
conveniently prepared by the slow addition of 2 equiv of trifluoromethanesulfonic acid to a stirring mixture of chlorodiisopropylsilane, followed by direct distillation of the product from the reaction flask to yield the product as a pale yellow oil.
-

Yield:85272-30-6 77%

Reaction Conditions:

for 2 h;Heating;

References:

Corey, E. J.;Hopkins, Paul B. [Tetrahedron Letters,1982,vol. 23,# 47,p. 4871 - 4874]

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