DIISOBUTYLALUMINUM CHLORIDE synthesis
- Product Name:DIISOBUTYLALUMINUM CHLORIDE
- CAS Number:1779-25-5
- Molecular formula:C8H18AlCl
- Molecular Weight:176.66
7446-70-0
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1779-25-5
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Yield:-
Reaction Conditions:
in diethyl ether;tolueneall manipulations under dry, O2 free N2 atm.; AlCl3 dissolved in Et2O, soln. of iso-Bu3Al in toluene added at -78°C, allowed to warm to room temp., stirred and refluxed for for 3, stirred at room temp. for 48 h h;
References:
Schumann, Herbert;Dechert, Sebastian;Hummert, Markus;Lange, Katharina C. H.;Schutte, Stefan;Wassermann, Birgit C.;Koehler, Katrin;Eichhorn, Jens [Zeitschrift fur Anorganische und Allgemeine Chemie,2004,vol. 630,# 8-9,p. 1196 - 1204]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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1191-15-7
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86050-32-0
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1779-25-5
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$45.00/10g