diethyl (3,3-dimethyl-2-oxobutyl)phosphonate synthesis
- Product Name:diethyl (3,3-dimethyl-2-oxobutyl)phosphonate
- CAS Number:814-16-4
- Molecular formula:C10H21O4P
- Molecular Weight:236.25
Yield:814-16-4 68%
Reaction Conditions:
with dipotassium peroxodisulfate;silver(I) acetate in water;N,N-dimethyl-formamide at 85; for 24 h;Inert atmosphere;Schlenk technique;chemoselective reaction;
References:
Li, Lili;Huang, Wenbin;Chen, Lijin;Dong, Jiaxing;Ma, Xuebing;Peng, Yungui [Angewandte Chemie - International Edition,2017,vol. 56,# 35,p. 10539 - 10544][Angew. Chem.,2017,vol. 129,# 35,p. 10675 - 10680,6] Location in patent:supporting information
66051-21-6
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