Diethyl 2-(cyanomethyl)malonate synthesis
- Product Name:Diethyl 2-(cyanomethyl)malonate
- CAS Number:17109-93-2
- Molecular formula:C9H13NO4
- Molecular Weight:199.2
Yield:17109-93-2 87%
Reaction Conditions:
Stage #1: diethyl malonatewith sodium hydride in tetrahydrofuran at 0; for 0.5 h;
Stage #2: cyanomethyl bromide in tetrahydrofuran at 20; for 17 h;Further stages.;
References:
Bowman;Bridge;Brookes;Cloonan;Leach [Journal of the Chemical Society. Perkin Transactions 1 (2001),2002,vol. 2,# 1,p. 58 - 68]
68922-87-2
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17109-93-2
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99841-91-5
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