Diethyl 1,3-acetonedicarboxylate synthesis
- Product Name:Diethyl 1,3-acetonedicarboxylate
- CAS Number:105-50-0
- Molecular formula:C9H14O5
- Molecular Weight:202.2
115996-74-2
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105-50-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 95percent sulfuric acid / 1 h 20 deg C, then 3 h 50 deg C
2: H2SO4 / H2O; CHCl3 / 1 h / 35 - 40 °C
References:
Zefirov, N. S.;Sadovaya, N. K.;Kombarova, S. V. [Journal of Organic Chemistry USSR (English Translation),1988,vol. 24,p. 101 - 104][Zhurnal Organicheskoi Khimii,1988,vol. 24,# 1,p. 116 - 119]
542-05-2
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105-50-0
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