Decanoyl chloride synthesis
- Product Name:Decanoyl chloride
- CAS Number:112-13-0
- Molecular formula:C10H19ClO
- Molecular Weight:190.71
334-48-5
630 suppliers
$6.00/25g
112-13-0
287 suppliers
$14.00/25g
Yield:112-13-0 100%
Reaction Conditions:
with oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane at 0 - 20; for 4 h;
Steps:
a a) Decanoyl chloride
To a cooled (0 °C) solution of decanoic acid (275 mg, 1.59 mmol) in DCM (8 mL) was added dropwise oxalyl chloride (0.56 mL, 6.39 mmol) and DMF (3 drops) and the mixture was stirred at room temperature for 4 h. The solvent was removed under reduced pressure to yield the title compound as a yellow oil (315 mg, 100%) which was used in the next synthetic step without further purification.
References:
ALMIRALL, S.A.;BACH TA?A, Jordi;ESTEVE TRIAS, Cristina;MIR CEPEDA, Marta WO2019/115405, 2019, A1 Location in patent:Page/Page column 48
142-62-1
471 suppliers
$13.80/2.5g
112-13-0
287 suppliers
$14.00/25g
108-31-6
859 suppliers
$13.47/50 G
60-32-2
605 suppliers
$5.00/10g
112-13-0
287 suppliers
$14.00/25g
79-37-8
478 suppliers
$17.67/10gm:
334-48-5
630 suppliers
$6.00/25g
112-13-0
287 suppliers
$14.00/25g
111-66-0
164 suppliers
$10.00/10 mL
112-13-0
287 suppliers
$14.00/25g