CYCLOHEXYL 2-PYRIDYL KETONE synthesis
- Product Name:CYCLOHEXYL 2-PYRIDYL KETONE
- CAS Number:6602-64-8
- Molecular formula:C12H15NO
- Molecular Weight:189.25
109-04-6
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2043-61-0
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6602-64-8
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Yield:6602-64-8 80%
Reaction Conditions:
Stage #1: 2-bromo-pyridinewith n-butyllithium in tetrahydrofuran;hexane at -78; for 0.5 h;
Stage #2: cyclohexanecarbaldehyde in tetrahydrofuran;hexane at -78; for 2 h;
Stage #3: with iodine;potassium carbonate in tert-butyl alcohol; for 14 h;Reflux;
References:
Ushijima, Sousuke;Dohi, Souya;Moriyama, Katsuhiko;Togo, Hideo [Tetrahedron,2012,vol. 68,# 5,p. 1436 - 1442] Location in patent:scheme or table
109-04-6
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$6.00/25g
2719-27-9
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$16.00/25mL
6602-64-8
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$45.00/10mg
70423-45-9
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6602-64-8
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100-70-9
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931-50-0
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$45.00/1g
6602-64-8
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$45.00/10mg
13737-05-8
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$155.00/1g
2719-27-9
355 suppliers
$16.00/25mL
6602-64-8
27 suppliers
$45.00/10mg