Cyclohexanecarbonitrile, 4-(1-methylethyl)- (9CI) synthesis
1synthesis methods
- Product Name:Cyclohexanecarbonitrile, 4-(1-methylethyl)- (9CI)
- CAS Number:191092-95-2
- Molecular formula:C10H17N
- Molecular Weight:151.25
Yield:191092-95-2 80%
Reaction Conditions:
Stage #1: 4-isopropyl-cyclohexanonewith potassium tert-butylate in tetrahydrofuran; for 0.333333 h;
Stage #2: [(p-methylphenyl)sulfonylmethyl]isonitrile in tetrahydrofuran; for 4 h;
References:
Mycka, Robert J.;Duez, Stephanie;Bernhardt, Sebastian;Heppekausen, Johannes;Knochel, Paul;Fleming, Fraser F. [Journal of Organic Chemistry,2012,vol. 77,# 17,p. 7671 - 7676]