cis-3-Hexenyl Acetate synthesis
- Product Name:cis-3-Hexenyl Acetate
- CAS Number:3681-71-8
- Molecular formula:C8H14O2
- Molecular Weight:142.2
928-96-1
476 suppliers
$14.00/1g
111-55-7
379 suppliers
$5.00/100g
3681-71-8
398 suppliers
$11.00/5g
Yield:3681-71-8 70%
Reaction Conditions:
with Candida antarctica lipase B immobilized on a macroporous acrylic resin at 40; for 19 h;Green chemistry;Enzymatic reaction;Temperature;
Steps:
General experiment for the optimised acetylation of alcohols, according to Scheme 2:
General procedure: Lipozyme 435 (2percent wt) was added to a solution of an alcohol (1 equiv) in EGDA (2 equiv).The reaction mixture was incubated in an orbital shaker (40 °C, 150 rpm) and the reaction progress wasmonitored by GC-FID (see Table 1).
References:
Puchl'Ová, Eva;Szolcsányi, Peter [Molecules,2020,vol. 25,# 14] Location in patent:supporting information
1516-17-2
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3681-71-8
398 suppliers
$11.00/5g
108-05-4
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$4.00/1000g
928-96-1
476 suppliers
$14.00/1g
3681-71-8
398 suppliers
$11.00/5g
928-96-1
476 suppliers
$14.00/1g
75-36-5
587 suppliers
$17.92/100G
3681-71-8
398 suppliers
$11.00/5g
928-96-1
476 suppliers
$14.00/1g
108-24-7
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$14.00/250ML
3681-71-8
398 suppliers
$11.00/5g