Cinnamyl chloride synthesis
- Product Name:Cinnamyl chloride
- CAS Number:21087-29-6
- Molecular formula:C9H9Cl
- Molecular Weight:152.62
82859-39-0
0 suppliers
inquiry
21087-29-6
126 suppliers
inquiry
Yield:21087-29-6 83%
Reaction Conditions:
with FeCl2(phen)3 in acetonitrile at 60; for 0.5 h;
Steps:
General procedure B. Fe(phen)3Cl2 mediated chlorination of iodoalkanes
General procedure: To a solution of iodoalkanes (0.12 mmol, 1.0 equiv) in CH3CN (1.2 mL) was added Fe(phen)3Cl2 (0.12 mmol, 1.0 equiv). After being stirred at 60 oC for the proper reaction time, solvent evaporation and silica gel column chromatography afforded the corresponding alkyl chloride product
References:
Hwang, Joon Young;Shin, Jung Ha;Seong, Eun Young;Kang, Eun Joo [Bulletin of the Korean Chemical Society,2018,vol. 39,# 5,p. 695 - 698] Location in patent:supporting information
4407-36-7
74 suppliers
$18.00/25g
21087-29-6
126 suppliers
inquiry
4393-06-0
32 suppliers
inquiry
21087-29-6
126 suppliers
inquiry
300-57-2
222 suppliers
$51.00/25mL
21087-29-6
126 suppliers
inquiry
3536-96-7
209 suppliers
$56.60/100ml
100-52-7
951 suppliers
$17.30/2g
21087-29-6
126 suppliers
inquiry