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39273-46-6

CHEMBRDG-BB 5550092 synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1) NaH / 1) DMF, 60-70 deg C, 1 h, 2) 80 deg C, overnight
2: NaOH / ethanol; H2O / 2 h / Heating

References:

DeRuiter, Jack;Swearingen, Blake E.;Wandrekar, Vinay;Mayfield, Charles A. [Journal of Medicinal Chemistry,1989,vol. 32,# 5,p. 1033 - 1038]