Celecoxib IMpurity 1 synthesis
3synthesis methods
- Product Name:Celecoxib IMpurity 1
- CAS Number:54779-81-6
- Molecular formula:C17H14F3N3O2S
- Molecular Weight:381.3722
Yield:54779-81-6 99 %Spectr.
Reaction Conditions:
with C16H22AuClN2;potassium tetrakis(pentafluorophenyl)borate in benzene-d6 at 20; for 24 h;Inert atmosphere;Schlenk technique;regioselective reaction;
References:
Hu, Xingbang;Martin, David;Bertrand, Guy [New Journal of Chemistry,2016,vol. 40,# 7,p. 5993 - 5996]