Boc-L-Cyclobutylglycine synthesis
- Product Name:Boc-L-Cyclobutylglycine
- CAS Number:155905-77-4
- Molecular formula:C11H19NO4
- Molecular Weight:229.27
116611-45-1
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155905-77-4
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 1) n-BuLi / 1) THF, -78 deg C, 15 min, 2) THF, -78 to -10 deg C
2: n-BuLi / tetrahydrofuran / -40 °C
3: 6percent Na-Hg, Na2HPO4 / methanol / 3 h / 0 - 20 °C
4: PPTS / ethanol / 6 h / 50 °C
5: CrO3, H2SO4 / 1 h / 0 - 20 °C
References:
Pauly, Regine;Sasaki, N. Andre;Potier, Pierre [Tetrahedron Letters,1994,vol. 35,# 2,p. 237 - 240]
![Carbamic acid, [1-[1-(phenylsulfonyl)cyclobutyl]-2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]-, 1,1-dimethylethyl ester, (1R)- (9CI)](/CAS/20210305/GIF/155905-73-0.gif)
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155905-77-4
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109-70-6
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155905-77-4
78 suppliers
$53.00/25mg