BENZYLTRIPHENYLPHOSPHONIUM IODIDE synthesis
- Product Name:BENZYLTRIPHENYLPHOSPHONIUM IODIDE
- CAS Number:1243-97-6
- Molecular formula:C25H22IP
- Molecular Weight:480.32
Yield:1243-97-6 97%
Reaction Conditions:
in dichloromethane at 20; for 12 h;
Steps:
2 Synthesis of benzyltriphenylphosphonium iodide
Triphenylphosphine 1.05 g (4 mmol)In 16 mL of dry dichloromethane was stirred at room temperature,After adding 1.31 g (6 mmol) of benzyl iodide to the solution,The mixture was further stirred at room temperature for 12 hours.After completion of the reaction, the solvent was distilled off, the residue obtained was washed with diethyl ether and the residue was vacuum-dried at 40 ° C. for 12 hours,1.87 g (yield 97%) of benzyltriphenylphosphonium iodide as a yellow solid was obtained.
References:
JP6172152,2017,B2 Location in patent:Paragraph 0142
100-44-7
659 suppliers
$13.50/250G
1243-97-6
20 suppliers
inquiry
111-78-4
164 suppliers
$10.00/25g
4885-02-3
194 suppliers
$10.00/1g
1754-88-7
5 suppliers
inquiry
![9-ethylbicyclo[3.3.1]nonan-9-ol](/CAS/GIF/21915-33-3.gif)
21915-33-3
5 suppliers
inquiry
1243-97-6
20 suppliers
inquiry