Antimycin A1b synthesis
- Product Name:Antimycin A1b
- CAS Number:116095-18-2
- Molecular formula:C28H40N2O9
- Molecular Weight:548.63
503-74-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
2: palladium on carbon; hydrogen / tetrahydrofuran / 2 h / 20 °C / 760.05 Torr / Darkness
3: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C
4: palladium on carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr
References:
Inai, Makoto;Nishii, Takeshi;Tanaka, Ayako;Kaku, Hiroto;Horikawa, Mitsuyo;Tsunoda, Tetsuto [European Journal of Organic Chemistry,2011,# 14,p. 2719 - 2729]
22621-41-6
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629-05-0
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35748-34-6
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116095-18-2
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17839-48-4
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