AKOS BC-0111 synthesis
- Product Name:AKOS BC-0111
- CAS Number:181513-08-6
- Molecular formula:C10H16N2O
- Molecular Weight:180.25
91761-27-2
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181513-08-6
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Yield:181513-08-6 85%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in methanol; under 1551.49 Torr;
Steps:
123.b
A solution of dimethyl-[2-(3-nitro-phenoxy)-ethyl]-amine (500mg, 2.38mmol) in methanol (20ml) was hydrogenated over 10% Pd-C at 30 psi until no further gas uptake was observed. The reaction mixture was then filtered over celite and concentrated to yield 3-(2-dimethylamino-ethoxy)-phenylamine (365mg, 85%) as viscous oil.
References:
WO2006/123145,2006,A1 Location in patent:Page/Page column 60
108-01-0
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4143-61-7
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591-27-5
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181513-08-6
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554-84-7
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181513-08-6
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13831-59-9
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181513-08-6
13 suppliers
$45.00/25mg