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ChemicalBook CAS DataBase List (2R,3R,4R,5R)-5-((benzoyloxy)Methyl)-3-Methyl-2-(5-Methyl-2,4-dioxo-3,4-dihydropyriMidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate
957535-53-4

(2R,3R,4R,5R)-5-((benzoyloxy)Methyl)-3-Methyl-2-(5-Methyl-2,4-dioxo-3,4-dihydropyriMidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate synthesis

1synthesis methods
alpha-D-erythro-Pentofuranous-2-ulose 1,3,5-tribenzoate

157037-56-4
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(2R,3R,4R,5R)-5-((benzoyloxy)Methyl)-3-Methyl-2-(5-Methyl-2,4-dioxo-3,4-dihydropyriMidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate

957535-53-4
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) CeCl3, 2.) DMAP, Et3N
2: 94 percent / bis(trimethylsilyl)acetamide, SnCl4 / acetonitrile / 3 h / Heating

References:

Harry-O'kuru, Rogers E.;Kryjak, Emily A.;Wolfe, Michael S. [Nucleosides and Nucleotides,1997,vol. 16,# 7-9,p. 1457 - 1460]