3-(2-AMINO-5-BROMO-PYRIDIN-3-YL)-ACRYLIC ACID METHYL ESTER synthesis
- Product Name:3-(2-AMINO-5-BROMO-PYRIDIN-3-YL)-ACRYLIC ACID METHYL ESTER
- CAS Number:912760-74-8
- Molecular formula:C9H9BrN2O2
- Molecular Weight:257.08
1072-97-5
694 suppliers
$9.00/1g
912760-74-8
26 suppliers
$140.00/50mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 0 - 20 °C
2: [Cp*RhCl2]2; silver hexafluoroantimonate; copper diacetate / 1,2-dichloro-ethane / 24 h / 120 °C / Schlenk technique; Inert atmosphere
3: hydrogenchloride / methanol; water / 3 h / 60 °C
References:
Zhou, Jun;Li, Bo;Hu, Fang;Shi, Bing-Feng [Organic Letters,2013,vol. 15,# 13,p. 3460 - 3463]
182344-63-4
28 suppliers
$58.00/1g
912760-74-8
26 suppliers
$140.00/50mg